1,2,3,4,5,6,7,8-八硫杂环辛烷合成路线 (共 272 条)
参考文献
B: B-Verb.3, 2.5.1.2, page 17 - 18
unveroeffentlich (1975)
反应条件
sulfur dioxide over 150°C;
参考文献
Angewandte Chemie, , vol. 67, p. 32 - 33
Na: SVol.3, 3.3.4, page 1186 - 1188
反应条件
catalyst: TiO2 (AOK-78-57) or VA-2 in gas catalytic conversion organosulfur compd. in gaseous reactor at temp. 220-600°C; vanadium-containing catalysts: titanium oxide catalyst AOK-78-57 or catalyst VA-2; gas analyzer EMG 20-1, MS;
参考文献
Russian Journal of Applied Chemistry, , vol. 81, # 10 p. 1725 - 1728
反应条件
catalyst: TiO2 (AOK-78-57) or VA-2 in gas catalytic conversion organosulfur compd. in gaseous reactor at temp. 220-600°C; vanadium-containing catalysts: titanium oxide catalyst AOK-78-57 or catalyst VA-2; gas analyzer EMG 20-1, MS;
参考文献
Russian Journal of Applied Chemistry, , vol. 81, # 10 p. 1725 - 1728
反应条件
in gas PF3 and SF4 (molar ratio 1.5:1) sealed in gold tube, heated at 324°C (2133 atm) for 24 h; detected by IR spectra;
参考文献
Inorganic Chemistry, , vol. 20, p. 1325 - 1326
反应条件
in neat (no solvent) heating under > 200 hPa SO2;
参考文献
Inorganic Chemistry, , vol. 36, # 24 p. 5570 - 5573
反应条件
in neat (no solvent) byproducts: N2; educt sealed under Ar heated up to 393 K under Ar at heating rate of 7.5 K/min; solid dissolved in CCl4, identified by TLC and with gas chromatograph;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 60, # 7 p. 2391 - 2394
反应条件
iron in gas on the surface if iron wire, 300°C, 11 h; trapped on KBr disc at -196°C, identified by i.r. spect. and elem. anal.;
参考文献
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), , p. 731 - 735
反应条件
in neat (no solvent) heating under > 200 hPa SO2;
参考文献
Inorganic Chemistry, , vol. 36, # 24 p. 5570 - 5573
参考文献
Inorganic Chemistry, , vol. 41, # 15 p. 3894 - 3900