1056246-49-1合成路线 （共 21 条）
反应条件
1.1: sodium hydroxide / water; dimethyl sulfoxide / 0 - 20 °C / Inert atmosphere 1.2: 0 - 20 °C / Inert atmosphere 2.1: hydrogenchloride / ethanol; water / 1 h / Reflux; Inert atmosphere 3.1: dihydrogen peroxide / 1 h / Cooling with ice; Inert atmosphere 4.1: sodium perchlorate monohydrate / methanol; water / 0.5 h / 0 °C / Inert atmosphere View Scheme
参考文献
Piel, Isabel; Pawelczyk, Marius D.; Hirano, Keiichi; Froehlich, Roland; Glorius, Frank
European Journal of Organic Chemistry, 2011 , # 28 p. 5475 - 5484
反应条件
(Et3NH)3PO4 1.) DMF, electrochemical reduction; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Carelli, Italo; Curulli, Antonella; Inesi, Achille; Zeuli, Errico
Journal of Chemical Research, Miniprint, 1990 , # 3 p. 620 - 644
反应条件
hydrogen iodide 0.0833333 h; Ambient temperature;
参考文献
Penso; Mottadelli; Albanese
Synthetic Communications, 1993 , vol. 23, # 10 p. 1385 - 1391
反应条件
triethylamine; potassium iodide in methanol T=20°C; 12 h; Irradiation;
参考文献
Chai, Wen; Takeda, Akihiro; Hara, Makoto; Ji, Shun-Jun; Horiuchi, C. Akira
Tetrahedron, 2005 , vol. 61, # 9 p. 2453 - 2463
反应条件
(Et3NH)3PO4 in N,N-dimethyl-formamide electrochemical reduction;
参考文献
Carelli, Italo; Curulli, Antonella; Inesi, Achille; Zeuli, Errico
Journal of Chemical Research, Miniprint, 1990 , # 3 p. 620 - 644
反应条件
(Et3NH)3PO4 in N,N-dimethyl-formamide electrochemical reduction;
参考文献
Carelli, Italo; Curulli, Antonella; Inesi, Achille; Zeuli, Errico
Journal of Chemical Research, Miniprint, 1990 , # 3 p. 620 - 644
反应条件
(Et3NH)3PO4 in N,N-dimethyl-formamide electrochemical reduction;
参考文献
Carelli, Italo; Curulli, Antonella; Inesi, Achille; Zeuli, Errico
Journal of Chemical Research, Miniprint, 1990 , # 3 p. 620 - 644
反应条件
(Et3NH)3PO4 in N,N-dimethyl-formamide electrochemical reduction;
参考文献
Carelli, Italo; Curulli, Antonella; Inesi, Achille; Zeuli, Errico
Journal of Chemical Research, Miniprint, 1990 , # 3 p. 620 - 644
反应条件
(Et3NH)3PO4 1.) DMF, electrochemical reduction; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Carelli, Italo; Curulli, Antonella; Inesi, Achille; Zeuli, Errico
Journal of Chemical Research, Miniprint, 1990 , # 3 p. 620 - 644
反应条件
hydrogenchloride; methanol; hydroxylamine; sodium acetate
参考文献
Belcher et al.
Journal of the Chemical Society, 1958 , p. 2743
