1056477-06-5合成路线 (共 120 条)
反应条件
1: 56 percent / anhydrous K2CO3 / acetone / Heating 2: 26 percent / aq. 1 N NaOH / Heating 3: 66 percent / 2,3-dichloro-5,6-dicyano-1,4-benzoquinone / benzene / Heating View Scheme
参考文献
Rodighiero; Palumbo; Magno; et al.
Journal of Heterocyclic Chemistry, 1986 , vol. 23, # 5 p. 1405 - 1410
反应条件
1: 62 percent / anhydrous K2CO3 / acetone / Heating 2: 56 percent / aq. 1 N NaOH / Heating 3: 36 percent / 2,3-dichloro-5,6-dicyano-1,4-benzoquinone / benzene / Heating View Scheme
参考文献
Rodighiero; Palumbo; Magno; et al.
Journal of Heterocyclic Chemistry, 1986 , vol. 23, # 5 p. 1405 - 1410
反应条件
1: 61 percent / anhydrous K2CO3 / acetone / 20 h / Heating 2: 72 percent / aq. 1 N NaOH / Heating 3: 49 percent / 2,3-dichloro-5,6-dicyano-1,4-benzoquinone / benzene / 20 h / Heating View Scheme
参考文献
Journal of Heterocyclic Chemistry, , vol. 23, # 5 p. 1405 - 1410
反应条件
1: 56 percent / anhydrous K2CO3 / acetone / Heating 2: 26 percent / aq. 1 N NaOH / Heating View Scheme
参考文献
Rodighiero; Palumbo; Magno; et al.
Journal of Heterocyclic Chemistry, 1986 , vol. 23, # 5 p. 1405 - 1410
反应条件
water T=125°C; 0.25 h; microwave irradiation;
参考文献
Utsukihara, Takamitsu; Nakamura, Hiroaki; Watanabe, Masashige; Akira Horiuchi
Tetrahedron Letters, 2006 , vol. 47, # 52 p. 9359 - 9364
反应条件
water; sodium chloride T=100°C; 0.25 h; microwave irradiation;
参考文献
Tetrahedron Letters, , vol. 47, # 52 p. 9359 - 9364
反应条件
hydrogenchloride; methanol; hydroxylamine; sodium acetate
参考文献
Belcher et al.
Journal of the Chemical Society, 1958 , p. 2743
反应条件
1: potassium carbonate 2: hydrochloric acid View Scheme
参考文献
Bergmann; Gierth
Justus Liebigs Annalen der Chemie, 1926 , vol. 448, p. 67
反应条件
(Et3NH)3PO4 1.) DMF, electrochemical reduction; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Carelli, Italo; Curulli, Antonella; Inesi, Achille; Zeuli, Errico
Journal of Chemical Research, Miniprint, 1990 , # 3 p. 620 - 644
反应条件
in 2-ethoxy-ethanol Bischler reaction; 0.166667 h; microwave irradiation;
参考文献
Chen, Jing; Hu, Yongzhou
Synthetic Communications, 2006 , vol. 36, # 11 p. 1485 - 1494