1056477-06-5合成路线 （共 120 条）
反应条件
1: 81 percent / NaOH / aq. ethanol / r.t., 30min., then reflux, 4h 2: 1. polyphosphoric acid; 2. Se powder / 1. 190-200 degC, 1.5h; 2. 300 degC, 8h View Scheme
参考文献
Tedjamulia, Marvin L.; Tominaga, Yoshinori; Castle, Raymond N.
Journal of Heterocyclic Chemistry, 1983 , vol. 20, p. 1485 - 1495
反应条件
(Et3NH)3PO4 in N,N-dimethyl-formamide electrochemical reduction;
参考文献
Carelli, Italo; Curulli, Antonella; Inesi, Achille; Zeuli, Errico
Journal of Chemical Research, Miniprint, 1990 , # 3 p. 620 - 644
反应条件
cerium(III) iodide in tetrahydrofuran 1 h; Ambient temperature;
参考文献
Fukuzawa, Shin-ichi; Tsuruta, Takuya; Fujinami, Tatsuo; Sakai, Shizuyoshi
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1987 , p. 1473 - 1478
反应条件
1: 82 percent / NaOH / aq. ethanol / r.t., 30min., then reflux, 4h 2: 78 percent / polyphosphoric acid / 1.5 h / 190 - 200 °C 3: 71 percent / Se powder / 8 h / 300 °C View Scheme
参考文献
Tedjamulia, Marvin L.; Tominaga, Yoshinori; Castle, Raymond N.
Journal of Heterocyclic Chemistry, 1983 , vol. 20, p. 1485 - 1495
反应条件
1: 84 percent / NaOH / aq. ethanol / r.t., 30min., then reflux, 4h 2: 80 percent / polyphosphoric acid / 1.5 h / 190 - 200 °C 3: 75 percent / Se powder / 8 h / 300 °C View Scheme
参考文献
Tedjamulia, Marvin L.; Tominaga, Yoshinori; Castle, Raymond N.
Journal of Heterocyclic Chemistry, 1983 , vol. 20, p. 1485 - 1495
反应条件
magnesium 1.) Et2O, 2.) Et2O, reflux; benzene, reflux, 8 h; Yield given. Multistep reaction;
参考文献
Hoshi, Nobuto; Sato, Kazuhiro; Uda, Hisashi; Hagiwara, Hisahiro
Journal of Chemical Research, Miniprint, 1984 , # 12 p. 3501 - 3596
参考文献
Hori, Mikio; Kataoka, Tadashi; Shimizu, Hiroshi; Imai, Eiji; Iwamura, Tatsunori; Maeda, Kaori
Chemical and Pharmaceutical Bulletin, 1986 , vol. 34, # 9 p. 3599 - 3605
反应条件
Nafion-TMS in chloroform 21 h; Heating;
参考文献
Carlson, Rolf; Gautun, Hanna; Westerlund, Andreas
Advanced Synthesis and Catalysis, 2002 , vol. 344, # 1 p. 57 - 60
反应条件
toluene-4-sulfonic acid in chloroform Heating;
参考文献
Wolff, J. Jens; Frenking, Gernot; Harms, Klaus
Chemische Berichte, 1991 , vol. 124, # 3 p. 551 - 561
反应条件
T=20°C; Substitution; acetalization; 20 h; Photolysis;
参考文献
Ji, Shun-Jun; Horiuchi, C. Akira
Bulletin of the Chemical Society of Japan, 2000 , vol. 73, # 7 p. 1645 - 1652
