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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
4-溴氯苯
合成路线
（共 741 条）
106-39-8
4-溴氯苯
+
75-97-8
频哪酮
→
反应条件
39489-86-6
1-(4-氯苯基)-3,3-二甲基-2-丁酮
反应条件
sodium t-butanolate; palladium diacetate in toluene T=85°C; 7 h; Product distribution; Further Variations:CatalystsTemperatures;
参考文献
Prashad, Mahavir; Liu, Yugang; Repic, Oljan
Advanced Synthesis and Catalysis, 2003 , vol. 345, # 4 p. 533 - 536
106-39-8
4-溴氯苯
+
75-97-8
频哪酮
→
反应条件
39489-86-6
1-(4-氯苯基)-3,3-二甲基-2-丁酮
反应条件
potassium tert-butylate; iron(II) chloride 1.) DMSO, RT, 20 min, 2.) DMSO, RT, 20 min; Yield given. Multistep reaction;
参考文献
Galli, Carlo; Gentili, Patrizia
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1993 , # 6 p. 1135 - 1140
106-39-8
4-溴氯苯
+
150-76-5
4-甲氧基苯酚
→
反应条件
40843-46-7
1-氯-4-(4-甲氧基苯氧基)苯
反应条件
copper(l) iodide; iron (III) acetylacetonate; potassium carbonate in N,N-dimethyl-formamide T=135°C; 12 h; Inert atmosphere;
参考文献
Liu, Xiaoyan; Zhang, Songlin
Synlett, 2011 , # 2 art. no. W15810ST, p. 268 - 272
106-39-8
4-溴氯苯
+
611-13-2
2-糠酸甲酯
→
反应条件
41019-40-3
5-(4-氯苯基)呋喃-2-羧酸甲酯
反应条件
potassium acetate; palladium diacetate in N,N-dimethyl acetamide T=130°C; 20 h; Inert atmosphere; regioselective reaction;
参考文献
Fu, Hai Yan; Doucet, Henri
European Journal of Organic Chemistry, 2011 , # 35 p. 7163 - 7173
106-39-8
4-溴氯苯
+
104-94-9
对甲氧基苯胺
→
反应条件
41018-73-9
(4-氯苯基)-(4-甲氧基苯基)-胺
反应条件
iron (III) acetylacetonate; copper (II) acetate monohydrate; potassium carbonate in N,N-dimethyl-formamide T=135°C; 20 h; Inert atmosphere;
参考文献
Liu, Xiaoyan; Zhang, Songlin
Synlett, 2011 , # 8 art. no. W00811ST, p. 1137 - 1142
106-39-8
4-溴氯苯
→
反应条件
41150-48-5
反应条件
copper T=200°C;
参考文献
Kimoto et al.
Yakugaku Zasshi, 1954 , vol. 74, p. 358
Chem.Abstr., 1955 , p. 5373
98-03-3
+
106-39-8
4-溴氯苯
→
反应条件
4153-45-1
反应条件
1: 1-chloro-4-bromobenzene With magnesium in tetrahydrofuran T=20°C; 1 h; 2: thiophene-2-carbaldehyde in tetrahydrofuran T=0 - 20°C; 2 h; 3: With 1,3-Diiodo-5,5-dimethyl-2,4-imidazolidinedione; potassium carbonate in tetrahydrofuran; tert-butyl alcohol 20 h; RefluxDarkness;
参考文献
Dohi, Souya; Moriyama, Katsuhiko; Togo, Hideo
Tetrahedron, 2012 , vol. 68, # 32 p. 6557 - 6564
110-91-8
+
106-39-8
4-溴氯苯
→
反应条件
70291-67-7
+
41605-90-7
反应条件
iron(III) oxide; L-proline; sodium t-butanolate in dimethyl sulfoxide T=135°C; 24 h;
参考文献
Quo, Diliang; Huang, He; Xu, Jinyi; Jiang, Hualiang; Liu, Hong
Organic Letters, 2008 , vol. 10, # 20 p. 4513 - 4516
106-39-8
4-溴氯苯
→
反应条件
5575-51-9
反应条件
1: 1-chloro-4-bromobenzene; magnesium in tetrahydrofuran T=0 - 20°C; 1 h; Heating / reflux; 2: bismuth(III) chloride in tetrahydrofuran T=0 - 20°C; Heating / reflux; 3: With water; ammonium chloride in tetrahydrofuran
参考文献
SANOFI-AVENTIS
Patent: US2007/142349 A1, 2007 ;
Location in patent: Page/Page column 12 ;
US 20070142349 A1
106-39-8
4-溴氯苯
→
反应条件
5578-98-3
反应条件
1.1: tris-(dibenzylideneacetone)dipalladium(0); di-tert-butyl-(2′-methyl-biphenyl-2-yl)-phosphane; potassium phosphate / ethylene glycol dimethyl ether / 14 h / 50 °C / |Inert atmosphere 2.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / acetonitrile / 2.5 h / 20 °C / |Inert atmosphere 3.1: NiCl6H2O; sodium tetrahydroborate / methanol / 0.5 h / 0 °C / |Cooling with ice 3.2: 2 h / 20 °C View Scheme
参考文献
Xu, Jingjing; Li, Xingyao; Wu, Jinlong; Dai, Wei-Min
Tetrahedron, 2014 , vol. 70, # 25 p. 3839 - 3846
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