1: ethyl-lithium With cerium(III) chloride in tetrahydrofuran T=-78°C; 2 h; 2: 1-morpholin-4-yl-hexan-1-one in tetrahydrofuran T=-78°C; 1.5 h; Further stages.;
参考文献
Badioli, Michele; Ballini, Roberto; Bartolacci, Massimo; Bosica, Giovanna; Torregiani, Elisabetta; Marcantoni, Enrico
The Journal of organic chemistry, 2002 , vol. 67, # 25 p. 8938 - 8942
perchloric acid; water; p-benozquinone; palladium diacetate in acetonitrile T=23°C; other temperature: 60 deg C; Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry, , vol. 55, # 9 p. 2924 - 2927