Krolevets, A. A.; Popov, A. G.; Adamov, A. V.; Martynov, I. V.
Doklady Chemistry, 1988 , vol. 303, p. 353 - 355
Dokl. Akad. Nauk SSSR Ser. Khim., 1988 , vol. 303, # 4 p. 876 - 878
water in tetrahydrofuran soln. warmed up from -30°C to room temp., stirred for 2 h, hydrolysis; chloroform added, washed with water, dried above Na2SO4, solvent and remainig oil distd., recrystn. of residue from ethanol gave triphenylstibane, elem. anal.;
sodium hydride in tetrahydrofuran; mineral oil T=0 - 20°C; Inert atmosphere;
参考文献
Serpell, Christopher J.; Cookson, James; Thompson, Amber L.; Brown, Christopher M.; Beer, Paul D.
Dalton Transactions, 2013 , vol. 42, # 5 p. 1385 - 1393
polysulfide; N(Et)4ClO4 in N,N-dimethyl-formamide in situ electrochemical generation of polysulfide from carbon-sulfur cathode; Title compound not separated from byproducts;
参考文献
Bulletin de la Societe Chimique de France, , vol. 133, # 3 p. 273 - 281
