in neat (no solvent) (N2); mixt. of Sn compd. and diene was freeze-pump-thaw degassed; sealed; wrapped with Al foil; heated at 100°C; NMR monitoring; not isolated;
参考文献
Zhou, Dong; Reiche, Clemens; Nag, Mrinmoy; Soderquist, John A.; Gaspar, Petet P.
Organometallics, 2009 , vol. 28, # 8 p. 2595 - 2608
1: With C44H44O6P2; (m-tolyl-O-)(p-tolyl-O-)2P; (m-tolyl-O-)2(p-tolyl-O-)P; tri(m-methylphenyl) phosphite; tri-p-tolyl phosphite T=99.84°C; 2: With Lewis acid T=109.84°C; Product distribution / selectivity;
