1,1,3,3-四乙氧基-2-甲基丙烷合成路线 （共 23 条）
参考文献
Klimko; Skoldinow
Zhurnal Obshchei Khimii, 1959 , vol. 29, p. 4027; engl. Ausg. S. 3987
反应条件
1: With boron trifluoride diethyl etherate
T=45°C; 1 h;
2: With sodium carbonate
T=45°C; 3 h;
参考文献
O'Sullivan, Paul T.; Buhr, Wilm; Fuhry, Mary Ann M.; Harrison, Justin R.; Davies, John E.; Feeder, Neil; Marshall, David R.; Burton, Jonathan W.; Holmes, Andrew B.
Journal of the American Chemical Society, 2004 , vol. 126, # 7 p. 2194 - 2207
参考文献
BASF Aktiengesellschaft
Patent: US4410733 A1, 1983 ;
反应条件
boron trifluoride-diethyl ether complex
参考文献
Rohm and Haas Company
Patent: US4028084 A1, 1977 ;
反应条件
zinc(II) chloride in diethyl ether
T=40 - 50°C; 2 h;
参考文献
Zaitsev; Dalinger; Starosotnikov; Kachala; Strelenko; Shkineva; Shevelev
Russian Journal of Organic Chemistry, 2005 , vol. 41, # 10 p. 1507 - 1515
反应条件
zinc(II) chloride in ethyl acetate
3 h; Ambient temperature;
参考文献
Makin, S. M.; Kruglikova, R. I.; Popova, T. P.; Tagirov, T. K.
Journal of Organic Chemistry USSR (English Translation), 1981 , vol. 17, # 4 p. 630 - 634
Zhurnal Organicheskoi Khimii, 1981 , vol. 17, # 4 p. 723 - 727
反应条件
iron(III) chloride; sodium hydrogencarbonate
1) 2 h, reflux; 2) 20 deg C, 2 h;
参考文献
Yatluk, Yu. G.; Suvorov, A. L.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1987 , vol. 23, # 3 p. 316 - 320
Khimiya Geterotsiklicheskikh Soedinenii, 1987 , vol. 23, # 3 p. 376 - 381
反应条件
1: SOCl2, Py / CH2Cl2
View Scheme
参考文献
Gerasimenko,A.V. et al.
Zhurnal Organicheskoi Khimii, 1966 , vol. 2, p. 1429 - 1433,1416 - 1419
反应条件
boron trifluoride diethyl etherate
参考文献
Wang, Chia-Lin J.; Salvino, J. M.
Tetrahedron Letters, 1984 , vol. 25, # 46 p. 5243 - 5246
参考文献
Gerasimenko,A.V. et al.
Zhurnal Organicheskoi Khimii, 1966 , vol. 2, p. 1429 - 1433,1416 - 1419
