4-(4-吡啶)苯甲酸甲酯合成路线 （共 17 条）
反应条件
sulfur in decalin Heating; Yield given;
参考文献
Shiao, Min-Jen; Chia, Win-Long; Shing, Tai-Li; Chow, Tahsin J.
Journal of Chemical Research, Miniprint, 1992 , p. 2101 - 2121
反应条件
1: tetrahydrofuran / 0.5 h / -55 °C 2: 1.) Zn, 2.) CuCN, LiCl 3: sulfur / decahydronaphthalene / Heating View Scheme
参考文献
Shiao, Min-Jen; Chia, Win-Long; Shing, Tai-Li; Chow, Tahsin J.
Journal of Chemical Research, Miniprint, 1992 , p. 2101 - 2121
反应条件
1: 1.) Zn, 2.) CuCN, LiCl 2: sulfur / decahydronaphthalene / Heating View Scheme
参考文献
Shiao, Min-Jen; Chia, Win-Long; Shing, Tai-Li; Chow, Tahsin J.
Journal of Chemical Research, Miniprint, 1992 , p. 2101 - 2121
反应条件
2,2'-azo-bisisobutyronitrile; tris-(trimethylsilyl)silane; acetic acid T=80°C; 32 h;
参考文献
Nunez, Araceli; Sanchez, Aranzazu; Burgos, Carolina; Alvarez-Builla, Julio
Tetrahedron, 2004 , vol. 60, # 29 p. 6217 - 6224
反应条件
1 h; Ambient temperatureIrradiation; Title compound not separated from byproducts;
参考文献
Ohkura, Kazue; Seki, Koh-ichi; Terashima, Masanao; Kanaoka, Yuichi
Tetrahedron Letters, 1989 , vol. 30, # 26 p. 3433 - 3436
反应条件
1: With sodium hydroxide; water in ethanol T=60°C; 2 h; 2: With hydrogenchloride in ethanol; water pH=6 - 7;
参考文献
Boehringer Ingelheim International GmbH
Patent: US2004/242572 A1, 2004 ;
Location in patent: Page/Page column 73 ;
反应条件
hydrogenchloride; hydrogen; platinum(IV) oxide in ethanol T=20°C; P=2250.23 Torr; 18 h;
参考文献
US2004/242572 A1, ;
Page/Page column 75 ;
