(+)-Ipc2B(烯丙基)硼烷合成路线 (共 14 条)
反应条件
in diethyl ether T=0 - 20°C; 1 h;
参考文献
Felpin; Girard; Vo-Thanh; Robins; Villieras; Lebreton
Journal of Organic Chemistry, 2001 , vol. 66, # 19 p. 6305 - 6312
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Felpin, Francois-Xavier; Lebreton, Jacques
Journal of Organic Chemistry, 2002 , vol. 67, # 26 p. 9192 - 9199
反应条件
in diethyl ether T=-78 - 20°C;
参考文献
Fraunhoffer, Kenneth J.; Bachovchin, Daniel A.; White, M. Christina
Organic Letters, 2005 , vol. 7, # 2 p. 223 - 226
反应条件
in diethyl ether T=-78 - 20°C; Brown allylboration; 1 h;
参考文献
Duffey, Matthew O.; LeTiran, Arnaud; Morken, James P.
Journal of the American Chemical Society, 2003 , vol. 125, # 6 p. 1458 - 1459
反应条件
1: BH3*SMe2 / tetrahydrofuran / 18 h / 20 °C 2: diethyl ether / 2 h / 0 °C 3: diethyl ether / 1 h / 20 °C View Scheme
参考文献
Crimmins, Michael T.; Haley, Matthew W.
Organic Letters, 2006 , vol. 8, # 19 p. 4223 - 4225
反应条件
in diethyl ether T=0 - 20°C;
参考文献
Zhan, Weiqiang; Jiang, Yi; Brodie, Peggy J.; Kingston, David G. I.; Liotta, Dennis C.; Snyder, James P.
Organic Letters, 2008 , vol. 10, # 8 p. 1565 - 1568
反应条件
1: diethyl ether / 2 h / 0 °C 2: diethyl ether / 1 h / 20 °C View Scheme
参考文献
Crimmins, Michael T.; Haley, Matthew W.
Organic Letters, 2006 , vol. 8, # 19 p. 4223 - 4225
参考文献
Hashihayata, Takashi; Sakoh, Hiroki; Goto, Yasuhiro; Yamada, Koji; Morishima, Hajime
Chemical and pharmaceutical bulletin, 2002 , vol. 50, # 3 p. 423 - 425
反应条件
1: Brown asymmetric allylation; Inert atmosphere; 2: With dihydrogen peroxide; sodium hydroxide Brown asymmetric allylation; Inert atmosphere;
参考文献
Cho, Hee Yeon; Morken, James P.
Journal of the American Chemical Society, 2010 , vol. 132, # 22 p. 7576 - 7577
反应条件
in diethyl ether T=-100°C; Addition; 1 h; Title compound not separated from byproducts;
参考文献
Synlett, , # 11 p. 1646 - 1648
反应条件
in diethyl ether T=-100°C; Addition; 1 h; Title compound not separated from byproducts;
参考文献
Felpin; Vo-Thanh; Robins; Villieras; Lebreton
Synlett, 2000 , # 11 p. 1646 - 1648