in tetrahydrofuran
CH3OSnBu3 was added to the mixt in THF at room temp. and stirred for 1 h (N2); quenched with 3N aq. HCl, extd. with hexane; dried over MgSO4, concd., column chromd. on silica gel (hexane);
参考文献
Ura, Yasuyuki; Hara, Ryuichiro; Takahashi, Tamotsu
Journal of Organometallic Chemistry, 2000 , vol. 611, # 1-2 p. 299 - 303
Pereyre, M.; Bellegarde, B.; Valade, J.
Comptes Rendus des Seances de l'Academie des Sciences, Serie C: Sciences Chimiques, 1967 , vol. 265, p. 939 - 941
Pereyre et al.
Journal of Organometallic Chemistry, 1968 , vol. 11, p. 97
Full Text View citing articles Show Details
Gmelin Handbook: Sn: Org.Comp.12, 1.4.1.1.1.5.2.2, page 97 - 113
byproducts: CH3COOCH3; slight excess of enolester; evapn. of CH3COOCH3; 25percent cis, 75percent trans;
参考文献
Pereyre et al.
Journal of Organometallic Chemistry, 1968 , vol. 11, p. 97
Full Text View citing articles Show Details
Gmelin Handbook: Sn: Org.Comp.12, 1.4.1.1.1.5.2.2, page 97 - 113
