反应条件
1: diethyl methoxycarbonylmethyl-phosphonate With n-butyllithium in tetrahydrofuran; hexane
T=-78°C; Wadsworth-Emmons reaction; 0.5 h; Inert atmosphere;
2: cyclohexanecarbaldehyde in tetrahydrofuran; hexane
T=-78 - 20°C; Wadsworth-Emmons reaction; Inert atmosphere; optical yield given as percent de;
参考文献
Claridge, Timothy D. W.; Davies, Stephen G.; Lee, James A.; Nicholson, Rebecca L.; Roberts, Paul M.; Russell, Angela J.; Smith, Andrew D.; Toms, Steven M.
Organic Letters, 2008 , vol. 10, # 23 p. 5437 - 5440
