3-(3-苯氧基苯基)-1-丙醇合成路线 (共 7 条)
反应条件
1: With sodium hydride in tetrahydrofuran; mineral oil T=0 - 20°C; 0.5 h; 2: With hydrogen; 5 palladium on charcoal in methanol
参考文献
The Board of Trustees of the University of Illinois
Patent: US2012/22024 A1, 2012 ;
Location in patent: Page/Page column 24 ;
US 20120022024 A1
反应条件
in tetrahydrofuran; water
参考文献
Imperial Chemical Industries PLC
Patent: US4791139 A1, 1988 ;
反应条件
in tetrahydrofuran; hexane; ethyl acetate
参考文献
Bristol-Myers Squibb Company
Patent: US5470845 A1, 1995 ;
反应条件
1: H2 / 5percent Pd/C / methanol / 1 h / Ambient temperature 2: LiAlH4 / tetrahydrofuran; diethyl ether / 1 h / Heating View Scheme
参考文献
Hashizume; Ito; Kanaya; Nagashima; Usui; Oshima; Kanao; Tomoda; Sunazuka; Kumagai; Omura
Chemical and Pharmaceutical Bulletin, 1994 , vol. 42, # 6 p. 1272 - 1278
反应条件
1: NaOMe / CH2Cl2 2: H2 / 5percent Pd/C / methanol / 1 h / Ambient temperature 3: LiAlH4 / tetrahydrofuran; diethyl ether / 1 h / Heating View Scheme
参考文献
Hashizume; Ito; Kanaya; Nagashima; Usui; Oshima; Kanao; Tomoda; Sunazuka; Kumagai; Omura
Chemical and Pharmaceutical Bulletin, 1994 , vol. 42, # 6 p. 1272 - 1278
反应条件
lithium aluminium tetrahydride in tetrahydrofuran; diethyl ether 1 h; Heating;
参考文献
Hashizume; Ito; Kanaya; Nagashima; Usui; Oshima; Kanao; Tomoda; Sunazuka; Kumagai; Omura
Chemical and Pharmaceutical Bulletin, 1994 , vol. 42, # 6 p. 1272 - 1278
反应条件
pyridine; phosphorus tribromide; sodium chloride; sodium hydrogencarbonate in diethyl ether; water
参考文献
FMC Corporation
Patent: US4808762 A1, 1989 ;