(η3-allyl)(η5-Cp)Pd; tetrabutylammomium bromide; triphenylphosphine; potassium hydroxide in water; toluene T=80°C; 10 h; Inert atmosphereSchlenk technique;

2-methyl-thiophene in 1,4-dioxane T=90°C; 0.583333 h; Inert atmosphereSchlenk techniqueSealed tube;

1.1: n-butyllithium / tetrahydrofuran; hexane / 2 h / -78 - 20 °C / |Inert atmosphere; |Schlenk technique 1.2: 8 h / -78 - 20 °C / |Inert atmosphere; |Schlenk technique 2.1: (η3-allyl)(η5-Cp)Pd; triphenylphosphine; tetrabutylammomium bromide; potassium hydroxide / toluene; water / 10 h / 80 °C / |Inert atmosphere; |Schlenk technique View Scheme