反应条件
in benzene byproducts: triphenylphosphine oxide; bubbling of O2 through C6H6 (15 min), addn. of the solid Rh complex, immediate forming of a brown soln., discontinuing of the O2 bubbling (1.5 h), closing the flask, cooling with ice (24 h), pptn. of a brickred compd.; filtration, washing (repeatedly with diethyl ether), drying (vac.); elem. anal.;
参考文献
Gazzetta Chimica Italiana, , vol. 118, # 6 p. 475 - 478
