ammonium formate; palladium on activated charcoal in methanol; water
T=20°C; 6.7 h;
参考文献
Nacario, Ruel; Kotakonda, Shailaja; Fouchard, David M. D.; Tillekeratne, L. M. Viranga; Hudson, Richard A.
Organic Letters, 2005 , vol. 7, # 3 p. 471 - 474
Marquet,A.; Jacques,J.
Bulletin de la Societe Chimique de France, 1960 , p. 166 - 169
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Blicke; Maxwell
Journal of the American Chemical Society, 1939 , vol. 61, p. 1780
in neat (no solvent)
heating under reflux (4 h), cooling; filtration of polymeric HNCS, further flash chromy. (SiO2, CH2Cl2 (30-40percent) in light petroleum);
参考文献
Dunn, Peter J.; Morris, Janet L.; Rees, Charles W.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 1745 - 1748