反应条件
in diethyl ether addn. of acrylonitrile to the Co compd. in ether under Ar and stirring at room temp. for 1 h; evapn. (vac.), dissolving in ether-hexane, chromy. on Al2O3, elution with ether-hexane, concn., cooling to -78°C, filtn., washing with pentane and drying (vac.); elem. anal.; exo-endo-mixture, identified by (1)H-NMR;
参考文献
Zeitschrift fuer Naturforschung, B: Chemical Sciences, , vol. 46, # 10 p. 1364 - 1376
