1: 3,3-dimethylbut-1-yne With n-butyllithium in tetrahydrofuran; hexane T=0°C; 0.25 h; 2: formic acid methyl ester in tetrahydrofuran; hexane T=0°C; Heating; 3: With water; ammonium chloride in tetrahydrofuran; hexane
参考文献
Bowling, Nathan P.; Burrmann, Nicola J.; Halter, Robert J.; Hodges, Jonathan A.; McMahon, Robert J.
Journal of Organic Chemistry, 2010 , vol. 75, # 19 p. 6382 - 6390
Mistryukov, E. A.; Korshevets, I. K.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1986 , vol. 35, # 3 p. 626 - 629
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1986 , # 3 p. 685 - 688
Mistryukov, E. A.; Korshevets, I. K.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1986 , vol. 35, # 3 p. 626 - 629
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1986 , # 3 p. 685 - 688
1: trans vinyl bromide With iodine; magnesium in tetrahydrofuran 1 h; Heating; 2: formic acid methyl ester in tetrahydrofuran T=20°C; 4 h; Further stages.;
