反应条件
formaldehyd in tetrahydrofuran Trans-MeOIr(CO)(PPh3)2 and paraformaldehyde are dissolved in THF and stirred ( 2 days, room temp.).; React. is monitored by IR. Removing of solvent yields yellow solid, chromy. on Florisil (eluant: THF/cyclohexane).;
参考文献
Organometallics, , vol. 7, p. 235 - 236