2,4,4-三甲基-1-戊烯合成路线 (共 303 条)
反应条件
sulfur dioxide in water T=51.1 - 165.5°C; P=4650.47 Torr; Product distribution / selectivity;
参考文献
US2011/65970 A1, ;
Page/Page column 4-5 ;
反应条件
in diethyl ether T=22°C; 3 h; Yield given. Yields of byproduct given;
参考文献
Journal of the American Chemical Society, , vol. 103, p. 1440
反应条件
organometallic tantalum hydride grafted onto silica T=150°C; P=750.075 Torr; 5 - 8.33333 h; Product distribution / selectivity;
参考文献
EP1932820 A1, ;
Page/Page column 15 ;
反应条件
W(H)3/Al2O3 T=150°C; P=750.075 Torr; 16 h;
参考文献
Chemical Communications, , # 18 p. 2523 - 2525
参考文献
Journal of the American Chemical Society, , vol. 64, p. 2971
反应条件
1: 91 percent / calcium hypochlorite, 3N HCl / CH2Cl2 / 2 h / 0 °C 2: 60 percent View Scheme
参考文献
Journal of Organic Chemistry, , vol. 46, # 21 p. 4111 - 4115
反应条件
in dimethylsulfoxide-d6 T=35 - 45°C; 2 h; Irradiationalso with tert-butylating reagents (copper or zinc complexes); reactivities relative to Ph2C=CHI, CH2=CHCH2Cl and HCCCH2Cl; MechanismProduct distribution;
参考文献
Journal of the American Chemical Society, , vol. 111, # 13 p. 4921 - 4927
反应条件
NiSO4 on γ-alumina; impregnated and calcined (catalyst of example 1a); palladium acetate on γ-alumina; impregnated and calcined (catalyst of example 1b); Intalox.(R). T=75 - 121°C; Gas phase; Product distribution / selectivity;
参考文献
WO2005/56503 A1, ;
Page/Page column 48-52 ;
反应条件
Purolite CT275 T=93°C; 96 - 167 h; Product distribution / selectivity;
参考文献
US2006/111598 A1, ;
Page/Page column 2-3 ;
参考文献
Journal of Organic Chemistry, , vol. 46, # 21 p. 4111 - 4115