2-甲基-2-[2-[2-[(2-甲基丙烷-2-基)氧基]乙氧基]乙氧基]丙烷合成路线 (共 3 条)
反应条件
1: tert-butyl alcohol With sodium in tetrahydrofuran T=20°C; 18 h; Inert atmosphere; 2: bis[2-(toluene-4-sulfonyloxy)ethyl] ether in tetrahydrofuran 18 h; Inert atmosphereReflux;
参考文献
Herbert, Simon A.; Castell, Dominic C.; Clayden, Jonathan; Arnott, Gareth E.
Organic Letters, 2013 , vol. 15, # 13 p. 3334 - 3337
反应条件
Amberlyst 15 T=50°C; P=10343.2 Torr; 6 h; Product distribution / selectivity;
参考文献
CPC CORPORATION, TAIWAN
Patent: US2011/160492 A1, 2011 ;
Location in patent: Page/Page column 2-3; sheet 2 ;
反应条件
Amberlyst 15 T=50°C; P=10343.2 Torr; 6 h; Vacuum distillation; Product distribution / selectivity;
参考文献
CPC CORPORATION, TAIWAN
Patent: US2011/160492 A1, 2011 ;
Location in patent: Page/Page column 3; sheet 9 ;