in toluene byproducts: NaF; dropping a soln. of amino-2,4,6-tri-t-butylphenyl-fluoroborane in toluene to a soln. of NaN(SiMe3)2 in toluene under N2 and refluxing for 8 h; distilling off the solvent and subliming the borolane from the residue, elem. anal.;
参考文献
Zeitschrift fuer Anorganische und Allgemeine Chemie, , vol. 619, p. 1474 - 1478