N-乙酰基-DL-环己基甘氨酸合成路线 （共 6 条）
反应条件
1-methyl-pyrrolidin-2-one; sulfuric acid; lithium bromide; palladium on activated charcoal T=100 - 120°C; P=45003.6 Torr; 12 h;
参考文献
Beller, Matthias; Moradi, Wahed A.; Eckert, Markus; Neumann, Helfried
Tetrahedron Letters, 1999 , vol. 40, # 24 p. 4523 - 4526
反应条件
hydrogenchloride; (R)-(+)-2-(Diphenylphosphino)-2′-methoxy-1,1′-binaphthyl; dipotassium tetrachloroplatinate in various solvent(s) T=120°C; P=45600 Torr; 15 h;
参考文献
Chemistry Letters, , vol. 32, # 2 p. 160 - 161
反应条件
RhH(CO)(triphenylphosphine)3; dicobalt octacarbonyl; hydrogen in ethyl acetate T=120°C; 4 h;
参考文献
Lin, J.J.; Knifton, John F.
Journal of Organometallic Chemistry, 1991 , vol. 417, # 1/2 p. 99 - 110
参考文献
Collection of Czechoslovak Chemical Communications, , vol. 31, p. 4563 - 4580
反应条件
N-methyl-pyrrolidine; sulfuric acid; water; triphenylphosphine; lithium bromide; palladium (II) bromide 1.) 70 deg C, 2.) 60 bar, 120 deg C, 12 h; Yield given. Multistep reaction;
参考文献
Synlett, , # 1 p. 108 - 110
反应条件
sodium hydroxide; acylase Amano 30000 from Aspergillus spp. (30 u/mg); water; cobalt(II) chloride T=37 - 40°C; 41 h;
参考文献
Beller, Matthias; Eckert, Markus; Geissler, Holger; Napierski, Bernd; Rebenstock, Heinz-Peter; Holla, E. Wolfgang
Chemistry - A European Journal, 1998 , vol. 4, # 5 p. 935 - 941
