2,2,5,5-四甲基己烷合成路线 （共 25 条）
反应条件
in toluene
T=19°C; 120 h;
参考文献
Diversi, Pietro; Ingrosso, Giovanni; Lucherini, Antonio; Lumini, Tito; Marchetti, Fabio; et al.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1988 , p. 133 - 140
反应条件
in pentane
14 h; Ambient temperature;
参考文献
Diversi, P.; Fasce, D.; Santini, R.
Journal of Organometallic Chemistry, 1984 , vol. 269, # 3 p. 285 - 294
反应条件
hydrogen; palladium/alumina
T=30°C; other alkynes; var. Pd/Al2O3 ratio, effect of triphenylphosphine addition; Product distributionMechanism;
参考文献
Siegel, Samuel; Hawkins, James Adrian
Journal of Organic Chemistry, 1986 , vol. 51, # 9 p. 1638 - 1640
参考文献
Darwent; Steacie
Journal of the American Chemical Society, 1940 , vol. 70, p. 2286
Full Text Show Details
Darwent; Steacie
Canadian Journal of Research, Section B: Chemical Sciences, 1949 , vol. 27, p. 181
反应条件
T=100 - 200°C; bei der Einw.von photochemisch angeregneten Quecksilberatomen;
参考文献
Darwent; Steacie
Cand.J.Res.<B>Chem.Abstr., 1947 , vol. 27, p. 181
Cand.J.Res.<B>Chem.Abstr., 1949 , p. 6516
反应条件
1: hydrogen chloride / anschliessend mit wss. Salzsaeure
2: diethyl ether; mercury (II)-chloride
View Scheme
参考文献
Lewina et al.
Zhurnal Obshchei Khimii, 1959 , vol. 29, p. 2236,2237;engl.Ausg.S.2202,2204
反应条件
diethyl ether; mercury dichloride
参考文献
Lewina et al.
Zhurnal Obshchei Khimii, 1959 , vol. 29, p. 2236,2237;engl.Ausg.S.2202,2204
反应条件
titanium tetrachloride
1) CH2Cl2, -40 to -30 deg C, 5 - 10 min, 2) CH2Cl2, 1 h; Yield given. Multistep reaction;
参考文献
Reetz, Manfred T.; Westermann, Juergen; Steinbach, Rainer
Journal of the Chemical Society, Chemical Communications, 1981 , # 5 p. 237 - 239
参考文献
Hennion; Banigan
Journal of the American Chemical Society, 1946 , vol. 68, p. 1203
参考文献
Whitmore et al.
Journal of the American Chemical Society, 1941 , vol. 63, p. 125
