1: 1-bromo-4-methoxy-benzene With diethylaluminium chloride; diisobutylaluminium hydride; magnesium; lithium chloride in tetrahydrofuran; n-heptane
T=25°C; 3 h;
2: With CuCN*2LiCl in tetrahydrofuran
T=-10°C; Michael addition; 0.0833333 h;
3: cyclohexenon With chloro-trimethyl-silane in tetrahydrofuran
T=-10 - 25°C; Michael addition;
参考文献
Gao, Hongjun; Knochel, Paul
Synlett, 2009 , # 8 p. 1321 - 1325
