7-乙酰氨基-1,2,4,5-四氢苯并[d]氮杂卓-3-羧酸乙酯合成路线 (共 1 条)
反应条件
1: ethyl 7-nitro-1,2,4,5-tetrahydro-3H-3-benzazepine-3-carboxylate With hydrogen; palladium 10 on activated carbon in ethanol T=20°C; P=3040.2 Torr; 16 h; 2: acetic acid in ethanol 165 h; Cooling with ice;
参考文献
ASTELLAS PHARMA INC.
Patent: US2011/269744 A1, 2011 ;
Location in patent: Page/Page column 22 ;
US 20110269744 A1