2-ó(4-氯苯)硫代苯甲醛合成路线 (共 3 条)
反应条件
1: p-chlorobenzenethiol With isopropylmagnesium chloride in tetrahydrofuran T=-78°C; 0.166667 h; 2: 2-iodophenyl 4-chlorobenzenesulfonate With isopropylmagnesium chloride in tetrahydrofuran T=-78 - 0°C; 3: N,N-dimethyl-formamide in tetrahydrofuran T=-40 - 20°C;
参考文献
Lin, Wenwei; Sapountzis, Ioannis; Knochel, Paul
Angewandte Chemie - International Edition, 2005 , vol. 44, # 27 p. 4258 - 4261
反应条件
potassium carbonate in acetonitrile Heating;
参考文献
Mansawat, Woraluk; Saengswang, Ittiphol; U-prasitwong, Palita; Bhanthumnavin, Worawan; Vilaivan, Tirayut
Tetrahedron Letters, 2007 , vol. 48, # 24 p. 4235 - 4238
反应条件
polymeric xylylene-ionene borohydride in methanol T=20°C; 0.5 h;
参考文献
Lakouraj, Moslem M.; Tajbakhsh, Mahmood; Mahalli, Majid S.
Monatshefte fur Chemie, 2008 , vol. 139, # 2 p. 117 - 123