2,3-二氨基苯甲酸甲酯合成路线 (共 23 条)
反应条件
hydrogenchloride in water
Reflux;
参考文献
McKinnell, R. Murray; Armstrong, Scott R.; Beattie, David T.; Fatheree, Paul R.; Long, Daniel D.; Marquess, Daniel G.; Shaw, Jeng-Pyng; Vickery, Ross G.
Bioorganic and Medicinal Chemistry Letters, 2013 , vol. 23, # 14 p. 4210 - 4215
反应条件
1: Et3N; DMAP / tetrahydrofuran / 25 °C
2: acetic acid / 120 °C
3: liq. NH3 / 80 °C / 30002.4 Torr
View Scheme
参考文献
Griffin; Srinivasan; White; Bowman; Calvert; Curtin; Newell; Golding
Pharmaceutical Sciences, 1996 , vol. 2, # 1 p. 43 - 47
反应条件
borane-pyridine complex in methanol
T=20°C;
参考文献
Beaulieu, Pierre L.; Boes, Michael; Bousquet, Yves; Fazal, Gulrez; Gauthier, Jean; Gillard, James; Goulet, Sylvie; LaPlante, Steven; Poupart, Marc-Andre; Lefebvre, Sylvain; McKercher, Ginette; Pellerin, Charles; Austel, Volkhard; Kukolj, George
Bioorganic and Medicinal Chemistry Letters, 2004 , vol. 14, # 1 p. 119 - 124