2-(三甲基硅氧基)苯甲醛合成路线 (共 6 条)
反应条件
niobium pentachloride in dichloromethane T=20°C; 0.5 h;
参考文献
Hou, Jun-Tao; Chen, Hong-Li; Zhang, Zhan-Hui
Phosphorus, Sulfur and Silicon and the Related Elements, 2011 , vol. 186, # 1 p. 88 - 93
参考文献
Journal of the American Chemical Society, , vol. 74, p. 1003,1005
反应条件
0.0833333 h; microwave irradiation;
参考文献
Mojtahedi; Saidi; Bolourtchian; Heravi
Phosphorus, Sulfur and Silicon and Related Elements, 2002 , vol. 177, # 2 p. 289 - 292
反应条件
montmorillonite K-10 Solid phase reaction; desilylation; 0.05 h; microwave irradiation;
参考文献
Mojtahedi, Mohammad M.; Saidi, Mohammad R.; Heravi, Majid M.; Bolourtchian, Mohammad
Monatshefte fur Chemie, 1999 , vol. 130, # 9 p. 1175 - 1178
反应条件
triethylamine in pyridine
2 h; Yield given. Yields of byproduct given;
参考文献
Cornforth, Sir John; Ming-hui, Du
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1991 , p. 2183 - 2187
反应条件
triphenylphosphine
1.) CH2Cl2, 0 deg C, 15 min, 2.) 7 min; Yield given. Multistep reaction;
参考文献
Barton, Thomas J.; Groh, Brian L.
Journal of Organic Chemistry, 1985 , vol. 50, # 2 p. 158 - 166