Carpenter, Yuen-Ying; Dyker, C. Adam; Burford, Neil; Lumsden, Michael D.; Decken, Andreas
Journal of the American Chemical Society, 2008 , vol. 130, # 46 p. 15732 - 15741
in n-heptane byproducts: CO; under Ar or N2, exclusion of light, stirred for 15 h at room temp.; observed by IR, removal of solvent in vac., extn. (toluene), VCl3 sepd. by filtration, soln. evapd. to dryness in vac. at room temp., washed with n-heptane (P2Ph4);
