in n-heptane byproducts: CO; under Ar or N2, exclusion of light, refluxed for 4 h; filtered hot (VCl3), partial evapn. of solvent, cooled at -78°C (P2Ph4);
tetra-n-butylammonium tetrafluoroborate; tetra-(n-butyl)ammonium iodide in various solvent(s) Ambient temperatureelektrochemical reaction, anode Mg bar, cathode stainless steel; var. solv.; Yields of byproduct given;
tetra-n-butylammonium tetrafluoroborate; tetra-(n-butyl)ammonium iodide in various solvent(s) Ambient temperatureelektrochemical reaction, anode Mg bar, cathode stainless steel; var. solv.;
Gillespie, Donal G.; Walker, Brian J.; Stevens, David; McAuliffe, Charles A.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 8 p. 1697 - 1703
