magnesium 1.) Et2O, 50 deg C, 3 h, 2.) overnight; Multistep reaction. Title compound not separated from byproducts;
参考文献
Ang, How Ghee; Chang, Betty; Kwik, Whei Lu
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1992 , # 14 p. 2161 - 2170
tetra-n-butylammonium tetrafluoroborate; tetra-(n-butyl)ammonium iodide in various solvent(s) Ambient temperatureelektrochemical reaction, anode Mg bar, cathode stainless steel; var. solv.; Yields of byproduct given;
参考文献
Folest, J. C.; Nedelec, J. Y.; Perichon, J.
Tetrahedron Letters, 1987 , vol. 28, # 17 p. 1885 - 1886
tetra-n-butylammonium tetrafluoroborate; tetra-(n-butyl)ammonium iodide in various solvent(s) Ambient temperatureelektrochemical reaction, anode Mg bar, cathode stainless steel; var. solv.; Yields of byproduct given;
参考文献
Folest, J. C.; Nedelec, J. Y.; Perichon, J.
Tetrahedron Letters, 1987 , vol. 28, # 17 p. 1885 - 1886
