反应条件
1: CH2Cl2 / Ambient temperature
2: Ac2O, NaOAc / Heating
3: 80 percent / LiEt3BH / tetrahydrofuran / -78 °C
4: 80 percent / PPTS / Ambient temperature
5: 70 percent / BF3*Et2O / CH2Cl2 / Ambient temperature
6: 1.) BH3*THF; 2.) 10 percent NaOH / 1.) THF, reflux; 2.) reflux
7: 1.) 5 percent NaOH; 2.) K2CO3 / 1.) CH2Cl2, 0 deg C to RT; 2.) MeOH, H2O, reflux
8: 77 percent / PDC, 4 Angstroem molecular sieves / CH2Cl2 / Ambient temperature
9: 60 percent / 5 percent KOH / ethanol / Heating
10: 87 percent / Bu3SnH, AIBN / benzene / Heating
11: 55 percent / LiAlH4 / tetrahydrofuran / Heating
View Scheme
参考文献
Suzuki, Hideaki; Aoyagi, Sakae; Kibayashi, Chihiro
Tetrahedron Letters, 1995 , vol. 36, # 6 p. 935 - 936
