1.1: diisopropylamine; n-BuLi / tetrahydrofuran; hexane / 4 h / -78 °C
1.2: 63 percent / tetrahydrofuran; hexane / 16 h / -78 - 23 °C
2.1: BH3*SMe2 / tetrahydrofuran / 72 h / 23 °C
2.2: 49 percent / aq. H2O2; NaOH / tetrahydrofuran / 48 h / 23 °C
View Scheme
参考文献
Ayala, Leticia; Lucero, Claudia G.; Antoinette, Jan; Romero; Tabacco, Sarah A.; Woerpel
Journal of the American Chemical Society, 2003 , vol. 125, # 50 p. 15521 - 15528
