2,4,6-三甲基吡啶合成路线 (共 205 条)
参考文献
Marvell; Magoon
Journal of the American Chemical Society, 1955 , vol. 77, p. 2542
反应条件
1: Raney nickel / Hydrogenation
2: potassium carbonate / 160 °C
3: benzene
View Scheme
参考文献
McElvain; Carney
Journal of the American Chemical Society, 1946 , vol. 68, p. 2592,2599
参考文献
Yanagita; Futaki
Journal of Organic Chemistry, 1956 , vol. 21, p. 949,953
反应条件
phenyllithium in diethyl ether
T=21°C; 2.5 h;
参考文献
Compagnon, Paul-Louis; Kimny, Tan
Bulletin des Societes Chimiques Belges, 1984 , vol. 93, # 1 p. 55 - 72
反应条件
phenyllithium in tetrahydrofuran
T=23°C; 23 h; further deprotonating agent, solvents, temperature, time; Product distribution;
参考文献
Compagnon, Paul-Louis; Kimny, Tan
Bulletin des Societes Chimiques Belges, 1984 , vol. 93, # 1 p. 55 - 72
反应条件
phenyllithium
1.) Et2O, reflux, 1 h; 2.) Et2O, r.t., 1 h; Yield given. Multistep reaction. Further byproducts given. Yields of byproduct given;
参考文献
Compagnon, Paul-Louis; Kimny, Tan; Gasquez, Francoise
Bulletin des Societes Chimiques Belges, 1981 , vol. 90, # 8 p. 803 - 816
反应条件
phenyllithium in diethyl ether
Product distribution;
参考文献
Compagnon, Paul-Louis; Kimny, Tan; Gasquez, Francoise
Bulletin des Societes Chimiques Belges, 1981 , vol. 90, # 8 p. 803 - 816
反应条件
in chloroform
T=25°C; enthalpie; Thermodynamic data;
参考文献
Chawla, B.; Mehta, S. K.
Journal of Physical Chemistry, 1984 , vol. 88, # 12 p. 2650 - 2655
反应条件
air; vanadium oxide-molybdenum oxide catalyst; water
T=380°C;
参考文献
Mathes; Sauermilch
Chemische Berichte, 1955 , vol. 88, p. 1276,1281
反应条件
T=380°C; Leiten ueber mit Vanadium(V)-oxid und Molybdaen(VI)-oxid impraegniertes Silicagel;
参考文献
Mathes; Sauermilch
Chemische Berichte, 1955 , vol. 88, p. 1276,1281