lithium in tetrahydrofuran inert atmosphere; treatment of Bu3SnCl with Li (0°C, 4 h), stepwise addn. of org. bromide during 90 min at 0 or 50°C; quenching with 10percent NH4Cl; NMR and mass spectroscopy; relative yields of products depending on reaction conditions;
参考文献
Nudelman, N. Sbarbati; Carro, Cecilia
Journal of Organometallic Chemistry, 1998 , vol. 563, # 1-2 p. 31 - 36
lithium in tetrahydrofuran inert atmosphere; treatment of Bu3SnCl with Li (0°C, 4 h), stepwise addn. of org. bromide (in presence of 1 atm CO) during 90 min at 50°C; quenching with 10percent NH4Cl; NMR and mass spectroscopy; relative yields of products depending on reaction conditions;
参考文献
Nudelman, N. Sbarbati; Carro, Cecilia
Journal of Organometallic Chemistry, 1998 , vol. 563, # 1-2 p. 31 - 36
