C54H80Cl2Fe2N2O4 in diethyl ether
T=22°C; 0.5 h; Inert atmosphere;
参考文献
UNIVERSITY OF PRINCE EDWARD ISLAND; GENESIS GROUP INC.; SHAVER, Michael, P.; KOZAK, Christopher, M.
Patent: WO2013/53046 A1, 2013 ;
Location in patent: Paragraph 00187-00191 ;
1: 2-bromo-naphthalene With magnesium in tetrahydrofuran
Inert atmosphereReflux;
2: 1-bromocyclohexane With (FeCl3)2(TMEDA)3 in tetrahydrofuran
T=20°C; Inert atmosphere;