1: in tetrahydrofuran
T=5 - 20°C; Brown hydroboration; Inert atmosphere;
2: With acetic acid in tetrahydrofuran
T=20 - 50°C;
3: With dihydrogen peroxide; sodium hydroxide in tetrahydrofuran; water
Cooling with ice;
参考文献
Mori, Kenji
Bioscience, Biotechnology and Biochemistry, 2009 , vol. 73, # 12 p. 2727 - 2730
palladium on activated charcoal; hydrogen
T=150°C; P=9000.9 Torr; Reagent/catalyst;
参考文献
Molinari, Valerio; Giordano, Cristina; Antonietti, Markus; Esposito, Davide
Journal of the American Chemical Society, 2014 , vol. 136, # 5 p. 1758 - 1761
