1: With n-butyllithium; 2-(dimethylamino)-ethanol in hexane T=0°C; 1 h; 2: With 1,2,2-trichloro-1,1,2-trichloro-ethane in tetrahydrofuran; hexane T=0°C; 1 h;
参考文献
Mathieu, Julien; Gros, Philippe; Fort, Yves
Chemical Communications, 2000 , # 11 p. 951 - 952
1: 3-Methylpyridine With fluorine in dichloromethane T=-78 - -50°C; 2: p-isocyanonitrobenzene in dichloromethane T=-50 - 0°C; 4 h; Further byproducts given. Title compound not separated from byproducts;
参考文献
Kiselyov, Alexander S.
Tetrahedron Letters, 2005 , vol. 46, # 13 p. 2279 - 2282