5,6-二氢苯并呋喃-7(4h)-酮合成路线 （共 9 条）
反应条件
tin(IV) chloride in dichloromethane T=0°C; 2 h;
参考文献
Walsh, Edward J.; Stone, Guy B.
Tetrahedron Letters, 1986 , vol. 27, # 10 p. 1127 - 1130
反应条件
sodium hydrogencarbonate 12 h; Ambient temperature;
参考文献
Seki, Maki; Sakamoto, Toshihiro; Suemune, Hiroshi; Kanematsu, Ken
Journal of the Chemical Society - Perkin Transactions 1, 1997 , # 11 p. 1707 - 1714
反应条件
1: With oxalyl dichloride; N,N-dimethyl-formamide in dichloromethane T=20°C; 2.25 h; Inert atmosphere; 2: With tin(IV) chloride in dichloromethane T=0°C; 0.75 h; Inert atmosphere;
参考文献
Miles, William H.; Connell, Katelyn B.; Ulas, Goezde; Tuson, Hannah H.; Dethoff, Elizabeth A.; Mehta, Varun; Thrall, April J.
Journal of Organic Chemistry, 2010 , vol. 75, # 20 p. 6820 - 6829
反应条件
1: (NH4)2[Ce(NO3)6] / methanol / -35 °C 2: Amberlyst 15 / toluene / 6 h / Heating 3: tetrabutylammonium fluoride View Scheme
参考文献
Miura, Masanori; Arai, Noriyoshi; Narasaka, Koichi
Bulletin of the Chemical Society of Japan, 1998 , vol. 71, # 6 p. 1437 - 1441
反应条件
in dimethyl sulfoxide T=20°C; Paterno-Buechi reaction; 6 h; UV-irradiation; Further byproducts.;
参考文献
Yabuno, Youhei; Hiraga, Yoshikazu; Abe, Manabu
Chemistry Letters, 2008 , vol. 37, # 8 p. 822 - 823
反应条件
in dimethyl sulfoxide T=20°C; Paterno-Buechi reaction; 6 h; UV-irradiation; optical yield given as percent destereoselective reaction;
参考文献
Yabuno, Youhei; Hiraga, Yoshikazu; Takagi, Ryukichi; Abe, Manabu
Journal of the American Chemical Society, 2011 , vol. 133, # 8 p. 2592 - 2604
反应条件
in toluene T=60°C; Paterno-Buechi reaction; 6 h; UV-irradiation; optical yield given as percent destereoselective reaction;
参考文献
Yabuno, Youhei; Hiraga, Yoshikazu; Takagi, Ryukichi; Abe, Manabu
Journal of the American Chemical Society, 2011 , vol. 133, # 8 p. 2592 - 2604
反应条件
in ethanol Inert atmosphereHeating;
参考文献
Montalban, Antonio Garrido; Baum, Sven M.; Cowell, Justin; McKillop, Alexander
Tetrahedron Letters, 2012 , vol. 53, # 33 p. 4276 - 4279
反应条件
in ethanol; water T=150°C; 36 h; Sealed vessel;
参考文献
Montalban, Antonio Garrido; Baum, Sven M.; Cowell, Justin; McKillop, Alexander
Tetrahedron Letters, 2012 , vol. 53, # 33 p. 4276 - 4279
