Swamy, K.C. Kumara; Chandrasekhar; Harland, John J.; Holmes, Joan M.; Day, Roberta O.; Holmes, Robert R.
Journal of the American Chemical Society, 1990 , vol. 112, # 6 p. 2341 - 2348
in Petroleum ether dropwise addn. of soln. of SnCl4 in petroleum ether (40-60°C) to soln. of 1-organo-organoxysilyl 2-phenylhydrazine (equimolar amts., 0 to -10°C, under dry nitrogen), ppt. filtered in a cold atm. of dry N2; washed, dried under reduced pressure; elem. anal.;
in Petroleum ether dropwise addn. of soln. of TiCl4 in petroleum ether (40-60°C) to soln. of 1-organo-organoxysilyl 2-phenylhydrazine (equimolar amts., 0 to -10°C, under dry nitrogen), ppt. filtered in a cold atm. of dry N2; washed, dried under reduced pressure; elem. anal.;
