(S)-(-)-1,1,2-三苯基-1,2-乙二醇合成路线 (共 36 条)
参考文献
Rebiere, F.; Riant, O.; Kagan, H.B.
Tetrahedron: Asymmetry, 1990 , vol. 1, # 3 p. 199 - 214
反应条件
1.1: lithium diisopropylamide / tetrahydrofuran / -78 - 0 °C 1.2: 51 percent / tetrahydrofuran / 2.58 h / -78 °C 2.1: hydrazine; KCN / methanol / 24 h / Heating View Scheme
参考文献
Journal of Organic Chemistry, , vol. 69, # 19 p. 6493 - 6495
反应条件
methanol in tert-butyl methyl ether 6 h; Heating / reflux; Product distribution / selectivity;
参考文献
US2006/194867 A1, ;
Page/Page column 9 ;
反应条件
1: 93 percent / 98 percent H2SO4 / 4 h / Heating 2: Mg / tetrahydrofuran / 16 h / Heating View Scheme
参考文献
Organic Preparations and Procedures International, , vol. 23, # 2 p. 173 - 180
反应条件
magnesium in tetrahydrofuran Grignard reaction; 16 h; Heating;
参考文献
Organic Preparations and Procedures International, , vol. 23, # 2 p. 173 - 180
参考文献
Journal of the Chemical Society, , vol. 107, p. 31
反应条件
lithium Multistep reaction;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 2317 - 2321
反应条件
iodine; magnesium 1.) THF, reflux, 3 h; 2.) THF, reflux, 3-5 h; Yield given. Multistep reaction;
参考文献
Chemische Berichte, , vol. 121, p. 397 - 406
反应条件
Yield given. Multistep reaction;
参考文献
Tetrahedron, , vol. 53, # 31 p. 10659 - 10670
反应条件
TDBPA(1+)*SbCl6(1-) in dichloromethane 1 h; Ambient temperature;
参考文献
Tetrahedron, , vol. 53, # 31 p. 10817 - 10826