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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
邻溴吡啶
合成路线
（共 1098 条）
109-04-6
邻溴吡啶
+
16883-69-5
N-苯甲酰甲基溴吡啶
→
反应条件
366-18-7
2,2'-联吡啶
反应条件
palladium diacetate; potassium carbonate; triphenylphosphine in toluene 12 h; RefluxInert atmosphere;
参考文献
Xu, Jimin; Cheng, Guolin; Su, Deyong; Liu, Yantao; Wang, Xinyan; Hu, Yuefei
Chemistry - A European Journal, 2009 , vol. 15, # 47 p. 13105 - 13110
109-04-6
邻溴吡啶
→
反应条件
5683-33-0
2-二甲氨基吡啶
+
366-18-7
2,2'-联吡啶
反应条件
1-(4-bromobenzyl)-3-(2-phenylethyl)benzimidazolium bromide; palladium diacetate; potassium carbonate in water; N,N-dimethyl-formamide T=120°C; Ullmann Condensation; 0.5 h; Microwave irradiation; Reagent/catalyst;
参考文献
Molecules, , vol. 18, # 4 p. 3712 - 3724
109-04-6
邻溴吡啶
+
98-80-6
苯硼酸
→
反应条件
1008-89-5
2-苯基吡啶
+
366-18-7
2,2'-联吡啶
反应条件
1-(4-bromobenzyl)-3-(4-chlorobenzyl)benzimidazolium chloride; palladium diacetate; potassium carbonate in water; N,N-dimethyl-formamide T=120°C; Suzuki-Miyaura Coupling; 0.166667 h; Microwave irradiation; Reagent/catalyst;
参考文献
Molecules, , vol. 18, # 4 p. 3712 - 3724
109-04-6
邻溴吡啶
→
反应条件
110-86-1
吡啶
+
5683-33-0
2-二甲氨基吡啶
+
366-18-7
2,2'-联吡啶
反应条件
1-(4-bromobenzyl)-3-(4-chlorobenzyl)benzimidazolium chloride; palladium diacetate; potassium carbonate in water; N,N-dimethyl-formamide T=120°C; Ullmann Condensation; 0.5 h; Microwave irradiation;
参考文献
Molecules, , vol. 18, # 4 p. 3712 - 3724
109-04-6
邻溴吡啶
+
100-63-0
苯肼
→
反应条件
1008-89-5
2-苯基吡啶
+
366-18-7
2,2'-联吡啶
+
92-52-4
联苯
反应条件
sodium hydroxide; mercury dichloride; palladium dichloride in methanol 6 h; Heating; Title compound not separated from byproducts;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 56, # 4 p. 1113 - 1115
110-89-4
哌啶
+
109-04-6
邻溴吡啶
→
反应条件
366-18-7
2,2'-联吡啶
+
68654-52-4
反应条件
5 Pd(II)/C(eggshell); triphenylphosphine in ethylene glycol T=100°C; Buchwald-Hartwig reaction; 0.5 h; Microwave irradiation;
参考文献
Yaunner, Ricardo S.; Barros, Jose C.; Da Silva, Joaquim F. M.
Applied Organometallic Chemistry, 2012 , vol. 26, # 6 p. 273 - 276
109-04-6
邻溴吡啶
+
98-80-6
苯硼酸
→
反应条件
1008-89-5
2-苯基吡啶
+
366-18-7
2,2'-联吡啶
+
92-52-4
联苯
反应条件
1-(4-bromobenzyl)-3-(2-phenylethyl)benzimidazolium bromide; palladium diacetate; potassium carbonate in water; N,N-dimethyl-formamide T=120°C; Suzuki-Miyaura Coupling; 0.166667 h; Microwave irradiation; Reagent/catalystSolvent;
参考文献
Molecules, , vol. 18, # 4 p. 3712 - 3724
109-04-6
邻溴吡啶
+
52770-24-8
→
反应条件
366-18-7
2,2'-联吡啶
反应条件
[1,3-bis(diphenylphosphino)propane]dichloro nickel (II) in tetrahydrofuran
参考文献
Tamao, K.; Kodama, S.; Nakajima, I.; Kumada, M.; Minato, A.; Suzuki, K.
Tetrahedron, 1982 , vol. 38, # 22 p. 3347 - 3354
109-04-6
邻溴吡啶
+
39978-69-3
→
反应条件
反应条件
sodium t-butanolate; bis(dibenzylideneacetone)-palladium(0) in 1,4-dioxane 8 h; Heating; Product distribution; Further Variations:Reagents;
参考文献
Averin, Alexei D.; Ranyuk, Elena R.; Golub, Svetlana L.; Buryak, Alexei K.; Savelyev, Evgenii N.; Orlinson, Boris S.; Novakov, Ivan A.; Beletskaya, Irina P.
Synthesis, 2007 , # 14 p. 2215 - 2221
109-04-6
邻溴吡啶
+
779989-20-7
→
反应条件
反应条件
2,2'-bis-(diphenylphosphino)-1,1'- binaphthyl; sodium t-butanolate; bis(dibenzylideneacetone)-palladium(0) in 1,4-dioxane 4 h; Heating; Product distribution; Further Variations:Reagents;
参考文献
Averin, Alexei D.; Ranyuk, Elena R.; Golub, Svetlana L.; Buryak, Alexei K.; Savelyev, Evgenii N.; Orlinson, Boris S.; Novakov, Ivan A.; Beletskaya, Irina P.
Synthesis, 2007 , # 14 p. 2215 - 2221
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