反应条件
in tetrahydrofuran
under dry N2 at 0°C, stirred soln. of (C6H5)3SnLi treated dropwise with soln. of 1,3-dibromopropane, kept at 25°C for 18 h, refluxed for 3 h; H2O added, evapd. (vac.), partitioned between H2O and CHCl3, org. phasedried, evapd. (vac.), crystd. (MeOH, then hexanes, then MeOH); elem. anal.;
参考文献
Ducharme, Yves; Latour, Stephan; Wuest, James D.
Organometallics, 1984 , vol. 3, p. 208 - 211
