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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
正戊烯
合成路线
（共 716 条）
60-35-5
乙酰胺
+
109-67-1
正戊烯
+
201230-82-2
→
反应条件
123-15-9
2-甲基戊醛
+
757959-95-8
+
1430826-26-8
反应条件
Rh(acac)(CO)2; hydrogen; toluene-4-sulfonic acid; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in methanol; diethylene glycol dimethyl ether T=100°C; P=37503.8 Torr; 8 h; Inert atmosphereSchlenk technique; Reagent/catalystSolvent; chemoselective reaction;
参考文献
ChemSusChem, , vol. 6, # 9 p. 1759 - 1773
109-67-1
正戊烯
+
201230-82-2
→
反应条件
66-25-1
正己醛
+
109-66-0
戊烷油
反应条件
[PtCl2(PhCN)2]; (4R,5R)-DIOP; tin(ll) chloride in benzene T=100°C; P=73550.8 Torr; 5 h; other alkenes, var. reagents, temp., pressure and time; Product distribution;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 54, # 11 p. 3438 - 3446
60-35-5
乙酰胺
+
109-67-1
正戊烯
+
201230-82-2
→
反应条件
105-30-6
2-甲基-1-戊醇
+
66-25-1
正己醛
+
111-27-3
正己醇
反应条件
Rh(acac)(CO)2; hydrogen; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in diethylene glycol dimethyl ether T=100°C; P=37503.8 Torr; 8 h; Inert atmosphereSchlenk technique; Catalytic behavior; Reagent/catalystSolvent; chemoselective reaction;
参考文献
ChemSusChem, , vol. 6, # 9 p. 1759 - 1773
60-35-5
乙酰胺
+
109-67-1
正戊烯
+
201230-82-2
→
反应条件
757959-95-8
+
1430826-26-8
反应条件
Rh(acac)(CO)2; hydrogen; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in diethylene glycol dimethyl ether T=100°C; P=37503.8 Torr; 4 h; Inert atmosphereSchlenk technique; Catalytic behavior; Reagent/catalystSolvent; chemoselective reaction;
参考文献
ChemSusChem, , vol. 6, # 9 p. 1759 - 1773
60-35-5
乙酰胺
+
109-67-1
正戊烯
+
201230-82-2
→
反应条件
7501-79-3
N-己基-乙酰胺
+
757959-95-8
+
1430826-26-8
反应条件
Rh(acac)(CO)2; hydrogen; toluene-4-sulfonic acid; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in diethylene glycol dimethyl ether T=100°C; P=37503.8 Torr; 4 h; Inert atmosphereSchlenk technique; Catalytic behavior; Reagent/catalystSolvent; chemoselective reaction;
参考文献
ChemSusChem, , vol. 6, # 9 p. 1759 - 1773
60-35-5
乙酰胺
+
109-67-1
正戊烯
+
201230-82-2
→
反应条件
123-15-9
2-甲基戊醛
+
7501-79-3
N-己基-乙酰胺
+
757959-95-8
+
1430826-26-8
反应条件
Rh(acac)(CO)2; hydrogen; toluene-4-sulfonic acid; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in diethylene glycol dimethyl ether T=100°C; P=37503.8 Torr; 4 h; Inert atmosphereSchlenk technique; Catalytic behavior; Reagent/catalystSolvent; chemoselective reaction;
参考文献
ChemSusChem, , vol. 6, # 9 p. 1759 - 1773
60-35-5
乙酰胺
+
109-67-1
正戊烯
+
201230-82-2
→
反应条件
105-30-6
2-甲基-1-戊醇
+
7501-79-3
N-己基-乙酰胺
+
757959-95-8
+
1430826-26-8
反应条件
Rh(acac)(CO)2; hydrogen; toluene-4-sulfonic acid; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in diethylene glycol dimethyl ether T=100°C; P=37503.8 Torr; 8 h; Inert atmosphereSchlenk technique; Catalytic behavior; Reagent/catalystSolvent; chemoselective reaction;
参考文献
ChemSusChem, , vol. 6, # 9 p. 1759 - 1773
109-67-1
正戊烯
+
10419-77-9
碘甲基膦酸二乙酯
→
反应条件
683-08-9
+
16165-66-5
反应条件
sodium tetrahydroborate; triethyl borane; tributyltin chloride in hexane; toluene T=-78°C; Yields of byproduct given;
参考文献
Balczewski; Pietrzykowski
Tetrahedron, 1997 , vol. 53, # 21 p. 7291 - 7304
110-89-4
+
109-67-1
正戊烯
+
201230-82-2
→
反应条件
7335-01-5
+
2591-86-8
反应条件
bis(1,5-cyclooctadiene)-rhodium(I) tetrafluoroborate; hydrogen; triphenylphosphine in methanol; toluene T=125°C; P=30002.4 Torr; 5 h; Product distribution; Further Variations:ReagentsSolventsPressures;
参考文献
Journal of the American Chemical Society, , vol. 125, # 34 p. 10311 - 10318
110-89-4
+
109-67-1
正戊烯
+
201230-82-2
→
反应条件
21901-99-5
+
7335-01-5
+
2591-86-8
反应条件
water; tetrairidium dodecacarbonyl in methanol T=150°C; P=41371.8 Torr; 0.5 h; other group 8 transition-metal catalysts; Product distribution;
参考文献
Journal of Organic Chemistry, , vol. 45, # 16 p. 3370 - 3372
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