反应条件
in tetrahydrofuran pentadienyllithium, from penta-1,4-diene and butyllithium, quenching with trimethyltin chloride at -70°C, the reaction mixt. pouring into satd. aq. NH4Cl soln., dilg. with H2O and extg. with pentane, hexamethylditin freezing out at -15°C; a mixture of isomers (E/Z=83.6:16.4) b.p. 50°C/10mm, identificated by elem. anal., NMR and mass spectra;
参考文献
Jones, Martin; Kitching, William
Australian Journal of Chemistry, 1984 , vol. 37, p. 1863 - 1880
