in tetrahydrofuran -78 deg C to room temp. then room temp., 30 min;
参考文献
Heras, Maria A. de las; Molina, Andres; Vaquero, Juan J.; Navio, Jose L. Garcia; Alvarez-Builla, Julio
Journal of Organic Chemistry, 1993 , vol. 58, # 21 p. 5862 - 5865
in tetrahydrofuran T=-5°C; 0.0833333 h; various amounts of nBuLi, other iodine compounds, various organolithium reagents; Product distributionMechanism;
1: n-butyllithium With anhydrous iron chloride in hexanes T=-78°C; 3 h; Inert atmosphere; 2: benzophenone in hexanes T=-78 - 25°C; 15 h; Inert atmosphere; 3: With hydrogenchloride; water in hexanes
参考文献
Eisch, John J.; Sohn, Jane U.; Rabinowitz, Edon J.
European Journal of Organic Chemistry, 2010 , # 15 p. 2971 - 2977
