hydroxylamine hydrochloride; sodium carbonate in ethanol; water T=55°C; 0.5 h; Sonication;
参考文献
Barros, Carlos Jonnatan Pimentel; De Freitas, Jucleiton J. Rufino; De Oliveira, Ronaldo N.; De Freitas Filho, Joao R.
Journal of the Chilean Chemical Society, 2011 , vol. 56, # 2 p. 721 - 722
Beim Gegenwart von Natriumaethylat unter Abdestillieren des Aethanols;
参考文献
Mallinckrodt Chem. Works
Patent: US2367632 , 1942 ;
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Wallingford; Jones; Homeyer
Journal of the American Chemical Society, 1942 , vol. 64, p. 577
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Mallinckrodt Chem. Works
Patent: US2342385 , 1941 ;
potassium phosphate buffer; lyophilized Zea mays nitrilase ZmNIT2 EC 3.5.5.1 in water T=30°C; pH=7.15; 14 h; Title compound not separated from byproducts;
1: With diisobutylaluminium hydride in toluene T=-20°C; 0.222222 h; Flow reactor; 2: With water; tartaric acid disodium salt in toluene T=0°C; chemoselective reaction;