in not given addn. of aq. soln. of Pb-acetate (buffered with NH4-citrate and NH3) to alkaline soln. of C4H10S;; pptn., drying to const. wt.;;
参考文献
Guryanova, E. N.; Kuzina, L. S.
Zhurnal Fizicheskoi Khimii, 1956 , vol. 30, p. 616 - 628
C. A., 1956 , p. 14292
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Gmelin Handbook: Pb: MVol.C4, 219, page 1700 - 1702
in neat (no solvent) byproducts: CH3OH; org. compd. addn. (syringe) to Sn-compd. (stirring) (exothermic rection provokes reflux of formed methanol after some min), mixt. stirring for 2h, MeOH vac. removal;
